Organometallic [Fe3O(OOCC6H5)6(H2O)3](NO3) as intercalant of bentonite

Hasja Paluta Utami, Donny Marihot Siburian

Abstract

Intercalation of organometalic compounds [Fe3O(OOCC6H5)6(H2O)](NO3)∙nH2O on bentonite by weight ratio of bentonite:organometallic  (1 : 1); (1 : 2); (1 : 3); and (1 : 4) has been carried out. The intercalation bentonite was characterized using FT-IR spectrophotometer, XRD and XRF anayses. Characterization using FT-IR spectrophotometer showed higher intensity of peak wavenumber  at 470.6 cm-1 for Fe3-O vibration on the ratio (1 : 3). While XRD characterization showed the shift of diffraction angle of 2θ was 5.2° and has bacal spacing of 16.8 Ǻ. In the XRF characterization, the intercalation process of organometalic compounds [Fe3O(OOCC6H5)6(H2O)](NO3)∙nH2O on bentonite was occurred optimally with percentage of metal oxide reached 71.75 %.


Keywords: intercalation, bentonite, organometallic, [Fe3O(OOCC6H5)6(H2O)](NO3)∙nH2O.

Authors

Hasja Paluta Utami
hasjapaluta8@gmail.com (Primary Contact)
Donny Marihot Siburian
Utami, H. P., & Siburian, D. M. (2017). Organometallic [Fe3O(OOCC6H5)6(H2O)3](NO3) as intercalant of bentonite. Science and Technology Indonesia, 1(1), 20–24. https://doi.org/10.26554/sti.2016.1.1.20-24
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