Structural Stability of Ni/Al Layered Double Hydroxide Supported on Graphite and Biochar Toward Adsorption of Congo Red
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Keywords:
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Ni/Al, Biochar, Graphite, Congo red, Structural Stability
Abstract
In this research, Ni/Al layered double hydroxide (LDH) was modified by using co-precipitation method to generate Ni/Al-graphite (Ni/Al-GF) and Ni/Al-biochar (Ni/Al-BC). The adsorbents were applied to remove Congo Red from aqueous solution. The obtained samples were characterized by using XRD, FTIR, BET and TG-DTA. The XRD diffraction pattern of Ni/Al LDH, Ni/Al-GF, and Ni/Al-BC presented the formation of composite with decreasing crystallinity. The surface area modified LDHs was higher than the pristine materials, which was obtained 15.106 m2/g, 21.595 m2/g and 438.942 m2/g for Ni/Al-LDH, Ni/Al-GF, Ni/Al-BC respectively. The adsorption of Congo Red on the materials was tested at dierent parameters and the results exhibited that Congo Red adsorption on LDHs were pseudo-first-order (PFO) kinetic, spontaneous, endothermic and followed Langmuir model. The adsorbents removed Congo Red by high performance stability with adsorption capacity was 116.297 mg/g for Ni/Al-GF and 312.500 mg/g for Ni/Al-BC. These adsorption capacity was higher than the pristine LDH (61.728 mg/g). The regeneration process which carried out for five cycles showed that Ni/Al-GF and Ni/Al-BC have stable structures as reuse adsorbents for Congo Red from aqueous solution.
References
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Aichour, A., H. Zaghouane-Boudiaf, F. B. M. Zuki, M. K. Aroua, and C. V. Ibbora (2019). Low-cost, biodegradable and highly effective adsorbents for batch and column fixed bed adsorption processes of methylene blue. Journal of Envi- ronmental Chemical Engineering, 7(5); 103409
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Annadurai, G., R. Juang, and D. Lee (2002). Use of cellulose- based wastes for adsorption of dyes from aqueous solutions. Journal of Hazardous Materials, 92(3); 263–274
Arabpour, A., S. Dan, and H. Hashemipour (2021). Prepara- tion and optimization of novel graphene oxide and adsorp- tion isotherm study of methylene blue. Arabian Journal of Chemistry, 14(3); 103003
Bernardo, M. P. and C. Ribeiro (2019). Zn–Al-based layered double hydroxides (LDH) active structures for dental restora- tive materials. Journal of Materials Research and Technology, 8(1); 1250–1257
Bharali, D. and R. C. Deka (2017). Adsorptive removal of congo red from aqueous solution by sonochemically synthe- sized NiAl layered double hydroxide. Journal of Environmen- tal Chemical Engineering, 5(2); 2056–2067
Bolbol, H., M. Fekri, and M. Hejazi-Mehrizi (2019). Lay- ered double hydroxide–loaded biochar as a sorbent for the
(2019). Synthesis of Positively Charged Polystyrene Mi- crospheres for the Removal of Congo Red, Phosphate, and Chromium(VI). ACS Omega, 4(4); 6669–6676
Daud, M., A. Hai, F. Banat, M. B. Wazir, M. Habib, G. Bharath, and M. A. Al-Harthi (2019). A review on the recent advances, challenges and future aspect of layered dou- ble hydroxides (LDH) – Containing hybrids as promising adsorbents for dyes removal. Journal of Molecular Liquids, 288; 110989
Demissie, H., G. An, R. Jiao, T. Ritigala, S. Lu, and D. Wang (2021). Modification of high content nanocluster-based co- agulation for rapid removal of dye from water and the mech- anism. Separation and Purification Technology, 259; 117845
Duan, C., X. Meng, C. Liu, W. Lu, J. Liu, L. Dai, W. Wang, W. Zhao, C. Xiong, and Y. Ni (2019). Carbohydrates-rich corncobs supported metal-organic frameworks as versatile biosorbents for dye removal and microbial inactivation. Car- bohydrate Polymers, 222; 115042
Forgacs, E., T. Cserháti, and G. Oros (2004). Removal of synthetic dyes from wastewaters: a review. Environment International, 30(7); 953–971
Gadekar, M. R. and M. M. Ahammed (2016). Coagula- tion/flocculation process for dye removal using water treat- ment residuals: modelling through artificial neural networks. Desalination and Water Treatment, 57(55); 26392–26400
Ghorai, S., A. K. Sarkar, A. B. Panda, and S. Pal (2013). Ef- fective removal of Congo red dye from aqueous solution using modified xanthan gum/silica hybrid nanocomposite as adsorbent. Bioresource technology, 144; 485–491
Guan, Y., J. Rao, Y. Wu, H. Gao, S. Liu, G. Chen, and F. Peng (2020). Hemicelluloses-based magnetic aerogel as an effi- cient adsorbent for Congo red. International Journal of Bio- logical Macromolecules, 155; 369–375
Harizi, I., D. Chebli, A. Bouguettoucha, S. Rohani, and A. Am- rane (2018). A New Mg–Al–Cu–Fe-LDH Composite to En- hance the Adsorption of Acid Red 66 Dye: Characterization, Kinetics and Isotherm Analysis. Arabian Journal for Science and Engineering, 44(6); 5245–5261
Hatami, H., A. Fotovat, and A. Halajnia (2018). Comparison of adsorption and desorption of phosphate on synthesized Zn-Al LDH by two methods in a simulated soil solution.Applied Clay Science, 152; 333–341
Hu, H., J. Liu, Z. Xu, L. Zhang, B. Cheng, and W. Ho (2019a).
Hierarchical porous Ni/Co-LDH hollow dodecahedron with excellent adsorption property for Congo red and Cr(VI) ions. Applied Surface Science, 478; 981–990
Hu, X., P. Li, X. Zhang, B. Yu, C. Lv, N. Zeng, J. Luo, Z. Zhang, J. Song, and Y. Liu (2019b). Ni-Based Catalyst Derived from NiAl Layered Double Hydroxide for Vapor Phase Catalytic Exchange between Hydrogen and Water. Nanomaterials, 9(12); 1688
Karami, Z., M. Jouyandeh, S. M. Hamad, M. R. Ganjali, M. Ag- hazadeh, L. Torre, D. Puglia, and M. R. Saeb (2019). Curing epoxy with Mg-Al LDH nanoplatelets intercalated with car- bonate ion. Progress in Organic Coatings, 136; 105278
Kartick, B., S. K. Srivastava, , and I. Srivastava (2013). Green Synthesis of Graphene. Journal of Nanoscience and Nanotech- nology, 13(6); 4320–4324
Kazeem, T. S., M. Zubair, M. Daud, and M. A. Al-Harthi (2020). Enhanced Removal of Eriochrome Black T Using Graphene/NiMgAl-Layered Hydroxides: Isotherm, Kinetic, and Thermodynamic Studies. Arabian Journal for Science and Engineering; 1–15
Keskin, E., U. Solmaz, G. Binzet, I. Gumus, and H. Arslan (2018). Synthesis, characterization and crystal structure of platinum (II) complexes with thiourea derivative ligands. European Journal of Chemistry, 9(4); 360–368
Khan, S. A., S. B. Khan, and A. M. Asiri (2016). Toward the design of Zn–Al and Zn–Cr LDH wrapped in activated carbon for the solar assisted de-coloration of organic dyes. RSC Advances, 6(86); 83196–83208
Khoshsang, H., A. Ghaffarinejad, H. Kazemi, Y. Wang, and H. Arandiyan (2018). One-pot synthesis of S-doped Fe 2 O 3/C magnetic nanocomposite as an adsorbent for anionic dye removal: equilibrium and kinetic studies. Journal of Nanostructure in Chemistry, 8(1); 23–32
Kristanto, G. A., A. R. Lamurvie, and W. Koven (2018). A Study of Compost as an Adsorbent for Congo Red Dye Removal Process. Reaktor, 17(4); 203
Lazzari, E., T. Schena, M. C. A. Marcelo, C. T. Primaz, A. N. Silva, M. F. Ferrão, T. Bjerk, and E. B. Caramão (2018). Classification of biomass through their pyrolytic bio-oil com- position using FTIR and PCA analysis. Industrial Crops and Products, 111; 856–864
Lei, C., M. Pi, C. Jiang, B. Cheng, and J. Yu (2017). Synthesis of hierarchical porous zinc oxide (ZnO) microspheres with highly efficient adsorption of Congo red. Journal of Colloid and Interface Science, 490; 242–251
Lellis, B., C. Z. Fávaro-Polonio, J. A. Pamphile, and J. C. Polonio (2019). Effects of textile dyes on health and the en- vironment and bioremediation potential of living organisms. Biotechnology Research and Innovation, 3(2); 275–290
Li, K., N. Kumada, Y. Yonesaki, T. Takei, N. Kinomura, H. Wang, and C. Wang (2010). The pH effects on the formation of Ni/Al nitrate form layered double hydroxides (LDHs) by chemical precipitation and hydrothermal method.
Materials Chemistry and Physics, 121(1-2); 223–229
Liu, R., H. Fu, H. Yin, P. Wang, L. Lu, and Y. Tao (2015a). A facile sol combustion and calcination process for the prepara- tion of magnetic Ni0.5Zn0.5Fe2O4 nanopowders and their adsorption behaviors of Congo red. Powder Technology, 274;
418–425
Liu, X., W. Li, N. Chen, X. Xing, C. Dong, and Y. Wang
(2015b). Ag–ZnO heterostructure nanoparticles with plasmon-enhanced catalytic degradation for Congo red un- der visible light. RSC Advances, 5(43); 34456–34465
Meili, L., P. Lins, C. Zanta, J. Soletti, L. Ribeiro, C. Dornelas, T. Silva, and M. Vieira (2019). MgAl-LDH/Biochar com- posites for methylene blue removal by adsorption. Applied Clay Science, 168; 11–20
Mohadi, R., , Z. Hanafiah, H. Hermansyah, and H. Zulkifli (2017). Adsorption of procion red and congo red dyes using microalgae Spirulina sp. Science and Technology Indonesia, 2(4); 102–104
Namasivayam, C. and D. Kavitha (2002). Removal of Congo Red from water by adsorption onto activated carbon pre- pared from coir pith, an agricultural solid waste. Dyes and pigments, 54(1); 47–58
Natarajan, S., V. Anitha, G. P. Gajula, and V. Thiagarajan (2020). Synthesis and Characterization of Magnetic Super- adsorbent Fe3O4-PEG-Mg-Al-LDH Nanocomposites for Ultrahigh Removal of Organic Dyes. ACS Omega, 5(7); 3181–3193
Oktriyanti, M. M., N. R. Palapa, R. Mohadi, and A. Lesbani (2019). Modification Of Zn-Cr Layered Double Hydroxide With Keggin Ion [?-SiW12O40] 4-AS Cr (VI) Adsorbent. Indonesian Journal of Environmental Management and Sustain- ability, 3(3); 93–99
Omer, O. S., B. H. Hussein, A. M. Ouf, M. A. Hussein, and A. Mgaidi (2018). An organified mixture of illite-kaolinite for the removal of Congo red from wastewater. Journal of Taibah University for Science, 12(6); 858–866
Pakhira, B., M. Ghosh, A. Allam, and S. Sarkar (2016). Carbon nano onions cross the blood brain barrier. RSC advances, 6(35); 29779–29782
Palapa, N. R., R. Mohadi, A. Rachmat, and A. Lesbani (2020). Adsorption Study of Malachite Green Removal from Aque- ous Solution Using Cu/M3+ (M3+=Al, Cr) Layered Double Hydroxide. Mediterranean Journal of Chemistry, 10(1); 33–45
Palapa, N. R., T. Taher, R. Mohadi, and A. Lesbani (2019). Removal of Anionic Direct Dye Using Zn/Al, Zn/Fe and Zn/Cr Layered Double Hydroxides Toward Interlayer Dis- tance. Science and Technology Indonesia, 4(3); 70
Pathania, D., A. Sharma, and Z.-M. Siddiqi (2016). Re- moval of congo red dye from aqueous system using Phoenix dactylifera seeds. Journal of Molecular Liquids, 219; 359–367
Popova, A. N. (2017). Crystallographic analysis of graphite by X-Ray diffraction. Coke and Chemistry, 60(9); 361–365
Puchana-Rosero, M., M. A. Adebayo, E. C. Lima, F. M. Machado, P. S. Thue, J. C. Vaghetti, C. S. Umpierres, and M. Gutterres (2016). Microwave-assisted activated carbonobtained from the sludge of tannery-treatment effluent plant for removal of leather dyes. Colloids and Surfaces A: Physico- chemical and Engineering Aspects, 504; 105–115
Radoor, S., J. Karayil, J. Parameswaranpillai, and S. Siengchin (2020). Removal of anionic dye Congo red from aqueous environment using polyvinyl alcohol/sodium alginate/ZSM- 5 zeolite membrane. Scientific Reports, 10; 1–15
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Authors
Siregar, P. M. S. B. N., Palapa, N. R., Wijaya, A., Fitri, E. S., & Lesbani, A. (2021). Structural Stability of Ni/Al Layered Double Hydroxide Supported on Graphite and Biochar Toward Adsorption of Congo Red. Science and Technology Indonesia, 6(2), 85–95. https://doi.org/10.26554/sti.2021.6.2.85-95
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